VHPS Lithium Battery Solvent Recovery & Distillation

Recover NMP and Electrolyte Solvents to Electronic Grade (≥99.95%). Achieve supply chain independence and cut energy costs by 40-60%.

  • 0%

    Methanol Purity

  • < 0 ppm

    Solvent Loss

  • 0 %

    Energy Reduction

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Lithium Battery & Solvent Challenges You’re Facing

As battery production scales, solvent recovery becomes the largest energy consumer and a critical quality control point.

Massive Energy Cost (NMP)

NMP’s high boiling point (202°C) makes traditional recovery extremely steam- and energy-intensive.
Impact: NMP recovery turns into a financial burden instead of a cost saving.

Strict Purity Requirements

Cathode materials cannot tolerate moisture above ~100 ppm or metal ions above ~1 ppm in recycled solvent.
Impact: Recovered solvent often fails “battery grade” specs and is downgraded or wasted.

Electrolyte Sensitivity

Carbonate solvents (DMC/EMC) degrade easily and require ultra-low water levels, often below 10 ppm.
Impact: Impurities and moisture lead to swelling cells and shorter cycle life.

Clogging from Slurry

Cleaning acetone from coating equipment carries binder and powders that quickly foul trays and packing.
Impact: Conventional distillation suffers frequent fouling, downtime and cleaning.

Environmental Compliance

NMP emissions and NMP-containing wastewater face increasingly strict occupational and discharge limits.
Impact: Non-compliance risks fines, production curtailment or plant shutdown.

Supply Chain Volatility

Virgin NMP and carbonate solvent prices fluctuate with market and feedstock conditions.
Impact: Lack of internal recycling creates cost unpredictability.

The Cost of Inefficient Processing

High NMP Expense

Virgin solvent procurement drains manufacturing profit margins.

Battery Defects

Trace moisture and metals reduce battery cycle life.

Carbon Intensity

High-energy recovery prohibits "Green Battery" certification.

The VHPS Advantage: Hypergravity + Heat Pump

A revolutionary "Five-in-One" synergy of High Gravity (HiGee), Energy Looping, and Intelligent Control.
  • Electronic-Grade Separation

    Generates a centrifugal force field to achieve deep dehydration and metal ion removal (< 1 ppm).

    Increases mass transfer rate by 1-3 orders of magnitude.

  • Heat-Pump Energy Integration

    Recycles latent heat efficiently, making the recovery of high-boiling NMP (202°C) economically viable.

    Reduces energy consumption by 40-60% compared to conventional columns

  • Anti-Clogging Flow Design

    Wide channels and high shear forces handle cleaning wastes containing slurry particles without fouling.

    Continuous operation with high-solid content fluids. 

Technical Specifications

Capacity Range
0.5 – 5 t/h
Product Purity
up to ≥99.5%
Solvent Recovery Rate
≥98–99%
Temperature Range
typically 40–160°C
Operating Pressure
typically 50–500 mbar
Typical Services
NMP recovery, electrolyte solvent recovery, solvent dehydration, high-salt/high-F wastewater conditioning
Typical Solvents
NMP, DMC, EMC, DEC, EC, PC, ethanol, methanol, IPA and other polar solvents

Performance Comparison

Get Technical Datasheet

Proven Lithium Battery & Materials Applications

From cathode coating to electrolyte filling, we provide total solvent management.

  • Multiple stainless steel process tanks and piping with overhead walkways and lighting inside a modern industrial production facility

    NMP Recovery from Cathode Coating

    Recovery and purification of NMP from cathode slurry mixing and dryer exhaust condensate, reducing fresh NMP demand.

    Industries:

    • NMP Recovery

    • Cathode Coating

    • VOC Reduction

    99.5%+

    NMP Purity

    30–50%

    Energy Savings

    ≥98–99%

    Recovery
  • Row of tall stainless steel process tanks with conical bottoms, access stairway and sanitary piping inside a bright, clean industrial production room

    Recycling & Black Mass Liquors

    Recovery of solvents from black mass leaching, washing and purification streams in battery recycling plants.

    Industries:

    • Recycling

    • Black Mass

    • Resource Recovery

    ≥95–99%

    Solvent Recovery

    0.5–3 t/h

    Capacity

    Lower

    Disposal Cost
  • Dimly lit corridor between large stainless steel process tanks with piping and overhead lines inside a modern industrial production facility

    VOC & NMP Emission Control

    Treatment of solvent-rich off-gas condensates and scrubber liquids to reduce NMP/VOC emissions and recover solvent.

    Industries:

    • VOC Control

    • NMP

    • Emissions

    ≥95–99%

    Solvent Recovery

    70–90%

    VOC Reduction

    30–50%

    Energy Savings
  • Wide view of a bright cleanroom production hall with stainless steel process vessels, piping and platforms on a glossy white floor

    Battery-Grade Solvent Dehydration

    Dehydration of NMP and carbonate solvents to very low water levels to meet battery-grade moisture specifications.

    Industries:

    • Dehydration

    • Low Moisture

    • Battery Grade

    Low

    Water

    0.5–3 t/h

    Capacity

    Stable

    Solvent Quality
  • Row of tall stainless steel process tanks with conical bottoms, access stairway and sanitary piping inside a bright, clean industrial production room

    Electrolyte Solvent Reclamation

    Reclamation of DMC, EMC, DEC, EC and PC from off-spec electrolyte, flushing solutions and blend changeovers.

    Industries:

    • Electrolyte

    • Solvent Reuse

    • OPEX Saving

    ≥99.5%

    Solvent Purity

    0.5–5 t/h

    Capacity

    Lower

    Fresh Solvent Use
  • Multiple tall stainless steel process tanks with conical bottoms, platforms and piping inside a bright, clean industrial production workshop

    High-Salt & Fluoride Wastewater

    Concentration and conditioning of lithium salt and fluoride-containing wastewater before further treatment or ZLD.

    Industries:

    • High-Salt

    • Fluoride

    • Wastewater

    30–50%

    COD Reduction

    0.5–5 t/h

    Capacity

    50–80%

    Volume Reduction
  • Typical Lithium Battery Solvents & Streams

    Key Li-ion battery solvents and process streams treatable by VHPS.
    Solvent / Stream
    Typical Source in Lithium Battery Manufacturing
    Key Issues / Pollutants
    VHPS Treatment Goal
    Example Performance
    NMP coating exhaust & wash liquors
    Cathode/anode coating and drying lines
    High boiling point (202°C), high energy, moisture and metal ions
    Recover electronic-grade NMP with low water/metals and lower energy use
    NMP ≥ 99.95%; water ≤ 100 ppm; metals ≤ 1 ppm; energy use ↓ 40–60%
    Electrolyte carbonates (DMC/DEC/EMC)
    Scrap electrolyte, off-spec electrolyte, flushing/flush batches
    Moisture sensitivity, degradation, acid formation
    Recover ultra-dry carbonate solvents without thermal decomposition
    Purity ≥ 99.95%; water ≤ 10 ppm; acid ≤ 10 μg KOH/g
    Acetone (and mixed) cleaning solvents
    Cleaning of coating machines, mixers, tanks and lines
    Binder and powder solids, high COD, fouling of conventional towers
    Regenerate cleaning solvent for reuse, remove solids and avoid clogging
    Purity ≥ 99.5%; solids removed; reusable fraction ↑; COD to WWTP ↓
    NMP-containing wastewater
    Scrubber water, rinses and wash water with low NMP content
    Low solvent concentration, high COD, discharge limits
    Concentrate NMP, recover clean water for reuse or ZLD schemes
    NMP concentrate ≥ 90%; volume reduction 50–80%; COD to WWTP reduced
    DMAC separator solvent loops
    Battery separator manufacturing (wet-process)
    High-boiling solvent, high energy, moisture control
    Recover DMAC for internal reuse and control water content
    DMAC ≥ 99.9%; water ≤ 200 ppm; energy use ↓ 30–50%
    High-salt / F⁻-containing process wastewater
    Cathode active material, etching/cleaning and precursor processes
    High TDS, fluorides (F⁻), scaling and difficult downstream treatment
    Concentrate high-salt/HF streams and protect downstream evaporators/WWTP
    Volume reduction 50–80%; improved treatability downstream
    Battery recycling black mass leach liquors
    Black mass leaching and washing in Li-ion battery recycling
    Dissolved metals, mixed solvents, high COD
    Separate solvents from metal-rich liquor, enrich metals and recover solvents
    High solvent recovery; metal concentration ↑; waste volume ↓
    Acetonitrile & specialty electrolyte solvents
    Formation/testing, electrolyte R&D and specialty formulations
    Toxicity, high solvent cost, purity specs
    Recover high-purity specialty solvents for reuse in battery production/R&D
    Purity ≥ 99.5%; recovery ≥ 95–99%; fresh solvent consumption reduced

    System Configuration & Compliance

    Engineered systems designed for methanol handling with full EU compliance and safety standards.

    VHPS-HGD-1000

    0.5-1.0 t/h
    Methanol capacity
    Footprint:
    8-12 m²
    Height:
    6.5 m
    Power:
    45-65 kW

    Typical Applications:

    Lab scale
    Pilot production
    Small batch

    VHPS-HGD-2500

    1.5-2.5 t/h
    Methanol capacity
    Footprint:
    12-16 m²
    Height:
    7.2 m
    Power:
    85-120 kW

    Typical Applications:

    Medium production
    API synthesis
    Fine chemicals

    VHPS-HGD-5000

    3.0-5.0 t/h
    Methanol capacity
    Footprint:
    16-22 m²
    Height:
    8.0 m
    Power:
    150-220 kW

    Typical Applications:

    Large scale
    Biodiesel
    Continuous operation

    Installation & Commissioning

    Engineering

    Detailed engineering package with P&IDs, equipment specifications, and installation drawings.

    Delivery

    Skid-mounted delivery with pre-assembled components and factory testing completed.

    Installation

    On-site installation supervision with utility connections and safety system verification.

    Commissioning

    Performance testing, operator training, and performance guarantee validation.
    Download Technical Specifications

    In Our Partners' Words

    Discover why industry leaders trust us to solve their most complex separation challenges.

    James Peterson

    Chief Technology Officer

    "Faced with a challenging separation and limited plant space, we turned to Superdistillation. Their Supergravity Heat-Pump Distillation (HG-HPD) system was the perfect solution. The compact design saved us from a costly expansion, and the performance is outstanding—we’re achieving higher purity while our energy costs have dropped by over 60%. It’s a truly innovative technology backed by world-class engineering support."

    FAQs

    Yes. VHPS hypergravity distillation is well suited for NMP recovery from mixer and dryer exhaust condensate, delivering high purity and high recovery while reducing VOC emissions and fresh NMP demand.

    Yes. VHPS can treat LiPF₆ electrolyte streams and carbonate solvents with controlled temperature and pressure. Proper design helps manage moisture and HF risks while recovering valuable solvents.

    In typical NMP and electrolyte solvent recovery service, VHPS heat-pump distillation can reduce energy use by about 30–50%, compared with conventional distillation or simple evaporation systems.

    VHPS units are delivered as compact skids that connect to dryer condensate tanks, solvent storage, wastewater and electrolyte handling systems. This allows you to add recovery and treatment capacity with minimal disruption to existing production.

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